饮用水中二甲基亚硝胺检测方法研究进展
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摘要
综述了饮用水中痕量级含氮消毒副产物二甲基亚硝胺(Dimethylnitrosamine,NDMA)的检测方法和检测技术。通过分析水样预处理方法以及各种检测手段,对现有检测技术进行比较,并重点针对浓缩倍数、固相萃取吸附剂以及色谱条件等关键问题进行研究,以期为饮用水中痕量级的NDMA检测提供科学的参考依据,为人们的饮用水卫生安全提供更高的保障。
It has introduced the detection methods and techniques of dimethylnitrosamine,which is a kind of trace nitrogen-containing disinfection by-products in drinking water. The existing detection techniques were compared by analyzing the pretreatment methods of water samples and test methods. And the key problems such as concentration multiple,solid-phase extraction adsorbent and chromatographic conditions were studied in order to provide scientific reference basis for the detection of NDMA in drinking water and provide higher guarantee for people's drinking water safety.
It has introduced the detection methods and techniques of dimethylnitrosamine,which is a kind of trace nitrogen-containing disinfection by-products in drinking water. The existing detection techniques were compared by analyzing the pretreatment methods of water samples and test methods. And the key problems such as concentration multiple,solid-phase extraction adsorbent and chromatographic conditions were studied in order to provide scientific reference basis for the detection of NDMA in drinking water and provide higher guarantee for people's drinking water safety.
引文
[1]杨磊.水中亚硝胺类消毒副产物生成规律及其前质去除方法研究[D].哈尔滨:哈尔滨工业大学,2010.
[2] Hrudey S E,Charrois J W A,Froese K L,et al. Occurrence of N-nitrosamines in Alberta public drinking water distribution systems[J]. J Environ Eng Sci,2007,6(1):103-114.
[3] Mitch W A,Sedlak D L. Formation of N-nitrosodimethylamine(NDMA)from dimethylamine during chlorination[J]. Environmental Science&Technology,2002,36(4):588-595.
[4]世界卫生组织.饮用水水质准则[S]. 4版.上海:上海交通大学出版社,2014.
[5] Clark R M,Boutin B K. Controlling disinfection by-products and microbial contaminants in drinking water[R].US:Environmental Protection Agency,2001:265-298.
[6]赵丽,师真,洪雪花,等.气相色谱-质谱法/MRM测定生活饮用水中N-二甲基亚硝胺(NDMA)的方法研究[J].湖北农业科学,2018,57(7):108-110,113.
[7]钱静汝,顾斌,安东.采用SPE-HPLC-MS/MS(APCI源)检测水中纳克级二甲基亚硝胺[J].给水排水,2017(3):24-28.
[8]李婷,鲜啟鸣. GC-EI/MS同时测定水中9种N-亚硝胺[J].中国测试,2013,39(4):40-44.
[9]陈祖辉.氮磷检测器气相色谱法测定水中痕量N-亚硝胺[J].分析化学,1981(6):7-11.
[10]罗茜,王东红,王炳一,等.超高效液相色谱串联质谱快速测定饮用水中9种N-亚硝胺的新方法[J].中国科学:化学,2011(1):82-90.
[11] Byun M W,Ahn H J,Kim J H,et al. Determination of volatile N-nitrosamines in irradiated fermented sausage by gas chromatography coupled to a thermal energy analyzer[J]. Journal of Chromatography A,2004,1054:403-407.
[12] Aygün S F,Uyanik A,Bati B. Adsorption of N-nitrosodiethylamine and N-nitrosodimethylamine on activated carbon:A pre-concentration procedure for gas chromatographic analysis[J]. Microchimica Acta,2004,146:279-283.
[13] Yurchenko S,Mlder U. N-Nitrosodimethylamine analysis in estonian beer using positive-ion chemical ionization with gas chromatography mass spectrometry[J]. Food Chem,2005,89:455-463.
[14]陈忠林,徐冰冰,齐虹,等.高效液相色谱测定水中痕量亚硝基二甲胺[J].中国给水排水,2007,23(8):84-87.
[15] Plum L M H,Reillllard M. Photochemical attenuaton of Nnitirosodimethylamine(NDMA)and ither nitrosamines in surface water[J]. Environment Science and Technology,2007,41(17):6170-6176.
[16]聂丽.固相萃取气相色谱/质谱测定饮用水中N-亚硝胺类消毒副产物的方法研究[D].武汉:华中科技大学,2015.
[17]许渝谨.固相萃取-气相色谱-正化学离子源质谱法检测水中9种亚硝胺类消毒副产物[D].青岛:青岛理工大学,2012.
[18]朱翔. N-亚硝胺的UPLC-MS/MS检测方法建立及强化混凝对城市污水厂二沉池出水中N-亚硝胺生成势的影响[D].西安:西安建筑科技大学,2014.
[19] Piumlee M H,López-Mesas M,Heidlberger A,et al. Nnitrosodimethylamine(NDMA)removal by reverse osmosis and UV treatment and analysis via LC-MS/MS[J].Water Res,2008,42(1/2):347-355.
[20] Planas C,Palacios O,Ventura F,et al. Analysis of nitrosamines in water by automated SPE and isotope dilution GC/HRMS-Occurrence in the different steps of a drinking water treatment plant,and in chlorinated samples from a reservoir and a sewage treatment plant effluent[J].Talanta,2008,76(4):906-913.
[2] Hrudey S E,Charrois J W A,Froese K L,et al. Occurrence of N-nitrosamines in Alberta public drinking water distribution systems[J]. J Environ Eng Sci,2007,6(1):103-114.
[3] Mitch W A,Sedlak D L. Formation of N-nitrosodimethylamine(NDMA)from dimethylamine during chlorination[J]. Environmental Science&Technology,2002,36(4):588-595.
[4]世界卫生组织.饮用水水质准则[S]. 4版.上海:上海交通大学出版社,2014.
[5] Clark R M,Boutin B K. Controlling disinfection by-products and microbial contaminants in drinking water[R].US:Environmental Protection Agency,2001:265-298.
[6]赵丽,师真,洪雪花,等.气相色谱-质谱法/MRM测定生活饮用水中N-二甲基亚硝胺(NDMA)的方法研究[J].湖北农业科学,2018,57(7):108-110,113.
[7]钱静汝,顾斌,安东.采用SPE-HPLC-MS/MS(APCI源)检测水中纳克级二甲基亚硝胺[J].给水排水,2017(3):24-28.
[8]李婷,鲜啟鸣. GC-EI/MS同时测定水中9种N-亚硝胺[J].中国测试,2013,39(4):40-44.
[9]陈祖辉.氮磷检测器气相色谱法测定水中痕量N-亚硝胺[J].分析化学,1981(6):7-11.
[10]罗茜,王东红,王炳一,等.超高效液相色谱串联质谱快速测定饮用水中9种N-亚硝胺的新方法[J].中国科学:化学,2011(1):82-90.
[11] Byun M W,Ahn H J,Kim J H,et al. Determination of volatile N-nitrosamines in irradiated fermented sausage by gas chromatography coupled to a thermal energy analyzer[J]. Journal of Chromatography A,2004,1054:403-407.
[12] Aygün S F,Uyanik A,Bati B. Adsorption of N-nitrosodiethylamine and N-nitrosodimethylamine on activated carbon:A pre-concentration procedure for gas chromatographic analysis[J]. Microchimica Acta,2004,146:279-283.
[13] Yurchenko S,Mlder U. N-Nitrosodimethylamine analysis in estonian beer using positive-ion chemical ionization with gas chromatography mass spectrometry[J]. Food Chem,2005,89:455-463.
[14]陈忠林,徐冰冰,齐虹,等.高效液相色谱测定水中痕量亚硝基二甲胺[J].中国给水排水,2007,23(8):84-87.
[15] Plum L M H,Reillllard M. Photochemical attenuaton of Nnitirosodimethylamine(NDMA)and ither nitrosamines in surface water[J]. Environment Science and Technology,2007,41(17):6170-6176.
[16]聂丽.固相萃取气相色谱/质谱测定饮用水中N-亚硝胺类消毒副产物的方法研究[D].武汉:华中科技大学,2015.
[17]许渝谨.固相萃取-气相色谱-正化学离子源质谱法检测水中9种亚硝胺类消毒副产物[D].青岛:青岛理工大学,2012.
[18]朱翔. N-亚硝胺的UPLC-MS/MS检测方法建立及强化混凝对城市污水厂二沉池出水中N-亚硝胺生成势的影响[D].西安:西安建筑科技大学,2014.
[19] Piumlee M H,López-Mesas M,Heidlberger A,et al. Nnitrosodimethylamine(NDMA)removal by reverse osmosis and UV treatment and analysis via LC-MS/MS[J].Water Res,2008,42(1/2):347-355.
[20] Planas C,Palacios O,Ventura F,et al. Analysis of nitrosamines in water by automated SPE and isotope dilution GC/HRMS-Occurrence in the different steps of a drinking water treatment plant,and in chlorinated samples from a reservoir and a sewage treatment plant effluent[J].Talanta,2008,76(4):906-913.