滤膜孔径分析常用方法
摘要
本文综述了显微成像图像分析法、标准颗粒过滤法、压汞法、氮气吸附法、泡点法等5种常用孔径分析方法的方法原理、优点、缺点及在滤膜孔径测量领域的应用。目前,并没有相关文献指出哪一种方法所测量的结果更准确,由于泡点法能准确测量孔喉直径,因此广泛应用于滤膜孔径大小及分布测量。
引文
[1]Agarwal C,Pandey A K,Pattyn D,et al.Neck-size distributions of through-pores in polymer membranes[J].Journal of Membrane Science,2012,415-416(10):608-615
[2]A.Hernández,Calvo J I,P.Prádanos,et al.Pore size distributions in microporous membranes.A critical analysis of the bubble point extended method[J].Journal of Membrane Science,1996,112(1):1-12
[3]Hayama M,K ohori F,Sak ai K.AFMobservation of small surf ace pores of hollow-f iber dialysis membrane using highly sharpened probe[J].Journal of Membrane Science,2002,197(1-2):243-249
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[6]陶继业.带静电促进的颗粒层过滤器高温煤气除尘研究[D].武汉大学,2005
[7]谢小军,黄翔,狄育慧.“燥灰纱”专用型驻极体空气过滤器的探讨[J].棉纺织技术,2005,33(8):33-35
[8]刘道清.空气过滤技术研究综述[J].环境科学与管理,2007,32(5):109-113
[9]纤维过滤机理及过滤器测试介绍[D],邹智胜,天津:天津大学,2004
[10]王红梅.压汞法测定多孔材料孔结构的误差[J].广州化工,2009,37(1):109-111
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[14]Venkataraman K,Choate W T,Torre E R,et al.Characterization studies of ceramic membranes.A novel technique using a coulter?Porometer[J].Journal of Membrane Science,1988,39(3):259-271
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[17]J.I.Calvo,P.Prádanos,A.Hernández,et al.Bulk and surf ace characterization of composite UK membranes,Atomic f orce microscopy,gas adsorption-desorption and liquid displacement techniques[J].Journal Membrane Science,1997,128:7-21
[18]International Organization f or Standardization.Permeable sintered metal materials-Determination of bubble test pore size:ISO 4003:1977[S].Switzerland:ISO,1977
[19]ASTM International.Standard test methods f or pore size characteristics of membrane f ilters by bubble point and mean f low pore test:ASTM F 316-03[S].West Conshohocken,PA:ASTM International,2011
[20]Li D,Frey M W,Yong L J.Characterization of nanof ibrous membranes with capillary f low porometry[J].Journal of Membrane Science,2006,286(1-2):104-114
[21]Shr estha A,Pellegrino J,Husson SM,et al.A modif ied por ometr y appr oach towards characterization of MF membranes[J].J o u r n a l o f M e m b r a n e S c i e n c e,2 0 12,421-422(Complete):145-153
[22]Schneider P,Uchytil P.Liquid expulsion permporometry f or characterization of porous membranes[J].Journal of Membrane Science,1994,95(1):29-38
[23]叶凌碧,刘大真,宇恒.孔径为1.2μm以下的微孔膜孔径测定方法[J].膜科学与技术,1983(1)
[2]A.Hernández,Calvo J I,P.Prádanos,et al.Pore size distributions in microporous membranes.A critical analysis of the bubble point extended method[J].Journal of Membrane Science,1996,112(1):1-12
[3]Hayama M,K ohori F,Sak ai K.AFMobservation of small surf ace pores of hollow-f iber dialysis membrane using highly sharpened probe[J].Journal of Membrane Science,2002,197(1-2):243-249
[4]Norman N Li,Anthony G.Fane,W.S.Winston Ho,Takeshi Matsuura.Advanced membrane technology and applications[M].USA:Wiley-AIChE,2008.320-344
[5]谢慧祎.高效空气过滤器及滤料杀菌效率评价方法的研究[D].天津大学,2006
[6]陶继业.带静电促进的颗粒层过滤器高温煤气除尘研究[D].武汉大学,2005
[7]谢小军,黄翔,狄育慧.“燥灰纱”专用型驻极体空气过滤器的探讨[J].棉纺织技术,2005,33(8):33-35
[8]刘道清.空气过滤技术研究综述[J].环境科学与管理,2007,32(5):109-113
[9]纤维过滤机理及过滤器测试介绍[D],邹智胜,天津:天津大学,2004
[10]王红梅.压汞法测定多孔材料孔结构的误差[J].广州化工,2009,37(1):109-111
[11]Kerch H M,Gerhardt R A,Grazul J L.Quantitative Electron Microscopic Investigation of the Pore Structure in 10:90 Colloidal Silica/Potassium Silicate Sol-Gels[J].Journal of the American Ceramic Society,1990,73(8):2228-2237
[12]谢晓永,唐洪明,王春华,等.氮气吸附法和压汞法在测试泥页岩孔径分布中的对比[J].天然气工业,2006,26(12):100-102
[13]Calvo J I,Hernández A,Prádanos P,et al.Pore Size Distributions in Microporous Membranes II.Bulk Characterization of Track-Etched Filters by Air Porometry and Mercury Porosimetry[J].Journal of Colloid&Interf ace Science,1995,176(2):467-478
[14]Venkataraman K,Choate W T,Torre E R,et al.Characterization studies of ceramic membranes.A novel technique using a coulter?Porometer[J].Journal of Membrane Science,1988,39(3):259-271
[15]Baklanov M R,Mogilnikov K P,Polovinkin V G,et al.Determination of pore size distribution in thin f ilms by ellipsometric porosimetry[J].Journal of vacuum science&technology.B,Microelectronics and nanometer structures:processing,measurement,and phenomena:an of f icial journal of the American Vacuum Society,2000,18(3):1385-1391
[16]Eiichi Kondoh,Mikhail R.Baklanov,Eric Lin,et al.Comparative study of pore size of lowdielectric-constant porous spin-on-glass f ilms using dif f erent method of nondestructive instrumentation[J].The Japan Society of Applied Physics,2001:323-326
[17]J.I.Calvo,P.Prádanos,A.Hernández,et al.Bulk and surf ace characterization of composite UK membranes,Atomic f orce microscopy,gas adsorption-desorption and liquid displacement techniques[J].Journal Membrane Science,1997,128:7-21
[18]International Organization f or Standardization.Permeable sintered metal materials-Determination of bubble test pore size:ISO 4003:1977[S].Switzerland:ISO,1977
[19]ASTM International.Standard test methods f or pore size characteristics of membrane f ilters by bubble point and mean f low pore test:ASTM F 316-03[S].West Conshohocken,PA:ASTM International,2011
[20]Li D,Frey M W,Yong L J.Characterization of nanof ibrous membranes with capillary f low porometry[J].Journal of Membrane Science,2006,286(1-2):104-114
[21]Shr estha A,Pellegrino J,Husson SM,et al.A modif ied por ometr y appr oach towards characterization of MF membranes[J].J o u r n a l o f M e m b r a n e S c i e n c e,2 0 12,421-422(Complete):145-153
[22]Schneider P,Uchytil P.Liquid expulsion permporometry f or characterization of porous membranes[J].Journal of Membrane Science,1994,95(1):29-38
[23]叶凌碧,刘大真,宇恒.孔径为1.2μm以下的微孔膜孔径测定方法[J].膜科学与技术,1983(1)