CTFA方法在检测化妆品防腐效果的适用性
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摘要
目的研究CTFA方法在检测国内不同化妆品防腐效果的适用性。方法采用美国化妆品、盥洗和香精联合会的测试方法(CTFA)人为将定量的菌种(细菌和真菌)分别加入到样品中,定期检测样品的菌落数,根据样品中的菌落数增减判定样品的防腐效果。结果 4类含有防腐剂的不同样品中有3类样品均能通过防腐实验, 1种类型样品不能通过防腐实验。结论 CTFA方法可以作为检测国内企业不同化妆品防腐效果的一种有效合理的方法,适用性良好。
Objective To study the applicability of CTFA method in detecting the antiseptic effect of different cosmetics in China. Methods Cosmetics, toiletries and fragrances association(CTFA) method was used to artificially add quantitative bacterial species(bacteria and fungi) to the samples, the number of bacterial colonies in the samples was regularly tested, and the antiseptic effect of the samples was determined according to the increase or decrease of the number of bacterial colonies in the samples. Results Totally 3 kinds of the 4 types of different samples containing preservatives could pass the anti-corrosion test, while one type of sample could not pass the anti-corrosion test. Conclusion CTFA method can be used as an effective and reasonable method to detect the antiseptic effect of different cosmetics in domestic enterprises, with good applicability.
Objective To study the applicability of CTFA method in detecting the antiseptic effect of different cosmetics in China. Methods Cosmetics, toiletries and fragrances association(CTFA) method was used to artificially add quantitative bacterial species(bacteria and fungi) to the samples, the number of bacterial colonies in the samples was regularly tested, and the antiseptic effect of the samples was determined according to the increase or decrease of the number of bacterial colonies in the samples. Results Totally 3 kinds of the 4 types of different samples containing preservatives could pass the anti-corrosion test, while one type of sample could not pass the anti-corrosion test. Conclusion CTFA method can be used as an effective and reasonable method to detect the antiseptic effect of different cosmetics in domestic enterprises, with good applicability.
引文
[1]郑萍,陈西平.化妆品微生物污染情况调查[J].中国卫生检验杂志,2009,19(10):2405-2406.Zheng P,Chen XP.Investigation on microbial contamination of cosmetics[J].Chin J Health Lab Technol,2009,19(10):2405-2406.
[2]许雅,曾转萍,吴宪毅.化妆品防腐剂抑菌和微生物污染关系的研究[J].中国卫生检验杂志,2005,(10):1201-1203.Xu Y,Zeng ZP,Wu XY.Study on the relationship between antiseptic and microbial contamination in cosmetics[J].Chin J Health Lab Technol,2005,(10):1201-1203.
[3]Muscatiello MJ.CTFA’s preservation guidelines:A historical perspective and review[J].Cosmet Toilet,1993,(108):53-59.
[4]Larsen WG,Jackson EM,Barker MO,et al.A primer on cosmetics.AADadvisory board,CTFA task force on cosmetics[J].J Am Acad Dermatol,1992,27(3):469-484.
[5]陈仪本,欧阳友生,陈娇娣,等.化妆品防腐体系的构建及其效能评价[J].日用化学品工业,2001,(4):42-46.Chen YB,Ouyang YS,Chen JD,et al.The construction of cosmetics anti-corrosion system and its efficacy evaluation[J].China Surf Deterg Cosmet,2001,(4):42-46.
[6]王永丽.几种化妆品的防腐挑战试验[J].广东化工,2015,(3):63-64.Wang YL.Anti-corrosion challenges of several cosmetics[J].Guangdong Chem Ind,2015,(3):63-64.
[7]范新雨,张太军,程双印,等.一种新的化妆品微生物挑战实验方法[J].香料香精化妆品,2007,(1):13-16.Fan XY,Zhang TJ,Cheng SY,et al.A new microbiological challenge experiment method for cosmetics[J].Flav Fragr Cosmet,2007,(1):13-16.
[8]邓志方,杜达安.化妆品防腐剂的使用概况及进展[J].华南预防医学,2000,(2):909-912.Deng ZF,Du DA.Overview and progress of the use of cosmetic preservatives[J].South China Prevent Med,2000,(2):909-912.
[9]仲瑶,姜雯.化妆品抑菌作用的初步研究[J].现代预防医学,2014,41(7):1274-1279.Zhong Y,Jiang W.Preliminary study on bacteriostatic effect of cosmetics[J].Mod Prev Med,2014,41(7):1274-1279.
[10]陆凌霞.用微生物挑战性试验对化妆品中常用防腐剂防腐效果的观察[J].广东卫生防疫,2000,(26):4.Lu LX.Observation on the antiseptic effect of common antiseptic in cosmetics by microorganism challenge test[J].Guangdong J Health Epid Prev,2000,(26):4.
[11]李素玉.化妆品防腐效能试验方法的选择[J].广州化工,2015,(15):148-149.Li SY.Selection of test methods for antiseptic efficacy of cosmetics[J].Guangzhou Chem Ind,2015,(15):148-149.
[12]关于发布化妆品安全技术规范(2015年版)的公告[EB/OL].[2018-7-18].http://scjg.fuzhou.gov.cn/zz/xxgk/fgwj/bljl/201807/t20180724_2535575.htm Notice on the issuance of technical specifications for safety of cosmetics(2015 edition)[EB/OL].[2018-7-18].http://scjg.fuzhou.gov.cn/zz/xxgk/fgwj/bljl/201807/t20180724_2535575.htm
[13]郭好洁,童贵忠,李娜.生物法检测化妆品中防腐剂的防腐效力观察[J].预防医学,2005,17(8):77.Guo HJ,Tong GZ,Li N.Observation on the antiseptic effect of preservatives in cosmetics by biological method[J].Prev Med,2005,17(8):77.
[14]张太军,陈朝茂,刘迪,等.化妆品微生物挑战性实验的优化[J].日用化学品科学,2013,36(5):26-29.Zhang TJ,Chen CM,Liu D,et al.Optimization of cosmetic microbial challenge experiments[J].Deterg Cosmet,2013,36(5):26-29.
[15]林惠芬,李斌,方惠英.用微生物挑战性试验评价化妆品防腐剂效果[J].日用化学工业,1999,(4):43-45.Lin HF,Li B,Fang HY.Evaluation of cosmetic preservative effect by microbiological challenge[J].China Surfact Deterg Cosmet,1999,(4):43-45.
[16]施昌松,蔡晓真,张洪广.化妆品中微生物与防腐体系的构建[J].日用化学品科学,2006,29(12):14-15.Shi CS,Cai XZ,Zhang HG.The construction of microorganism and anti-corrosion system in cosmetics[J].Deterg Cosmet,2006,29(12):14-15.
[17]庄孟芙,向立群,江俊华.山梨坦辛酸酯在个人护理产品中的防腐协同增效作用研究[J].中国洗涤用品工业,2017,(6):39-43.Zhuang MF,Xiang LQ,Jiang JH.Study on the antiseptic synergistic effect of sorbitan octanate in personal care products[J].China Clean Ind Assoc,2017,(6):39-43.
[18]张蓥.食品防腐中生物防腐剂的应用探究[J].食品安全导刊,2018,(6):112-113.Zhang Y.Research on the application of biological preservatives in food preservatives[J].China Food Saf Mag,2018,(6):112-113.
[2]许雅,曾转萍,吴宪毅.化妆品防腐剂抑菌和微生物污染关系的研究[J].中国卫生检验杂志,2005,(10):1201-1203.Xu Y,Zeng ZP,Wu XY.Study on the relationship between antiseptic and microbial contamination in cosmetics[J].Chin J Health Lab Technol,2005,(10):1201-1203.
[3]Muscatiello MJ.CTFA’s preservation guidelines:A historical perspective and review[J].Cosmet Toilet,1993,(108):53-59.
[4]Larsen WG,Jackson EM,Barker MO,et al.A primer on cosmetics.AADadvisory board,CTFA task force on cosmetics[J].J Am Acad Dermatol,1992,27(3):469-484.
[5]陈仪本,欧阳友生,陈娇娣,等.化妆品防腐体系的构建及其效能评价[J].日用化学品工业,2001,(4):42-46.Chen YB,Ouyang YS,Chen JD,et al.The construction of cosmetics anti-corrosion system and its efficacy evaluation[J].China Surf Deterg Cosmet,2001,(4):42-46.
[6]王永丽.几种化妆品的防腐挑战试验[J].广东化工,2015,(3):63-64.Wang YL.Anti-corrosion challenges of several cosmetics[J].Guangdong Chem Ind,2015,(3):63-64.
[7]范新雨,张太军,程双印,等.一种新的化妆品微生物挑战实验方法[J].香料香精化妆品,2007,(1):13-16.Fan XY,Zhang TJ,Cheng SY,et al.A new microbiological challenge experiment method for cosmetics[J].Flav Fragr Cosmet,2007,(1):13-16.
[8]邓志方,杜达安.化妆品防腐剂的使用概况及进展[J].华南预防医学,2000,(2):909-912.Deng ZF,Du DA.Overview and progress of the use of cosmetic preservatives[J].South China Prevent Med,2000,(2):909-912.
[9]仲瑶,姜雯.化妆品抑菌作用的初步研究[J].现代预防医学,2014,41(7):1274-1279.Zhong Y,Jiang W.Preliminary study on bacteriostatic effect of cosmetics[J].Mod Prev Med,2014,41(7):1274-1279.
[10]陆凌霞.用微生物挑战性试验对化妆品中常用防腐剂防腐效果的观察[J].广东卫生防疫,2000,(26):4.Lu LX.Observation on the antiseptic effect of common antiseptic in cosmetics by microorganism challenge test[J].Guangdong J Health Epid Prev,2000,(26):4.
[11]李素玉.化妆品防腐效能试验方法的选择[J].广州化工,2015,(15):148-149.Li SY.Selection of test methods for antiseptic efficacy of cosmetics[J].Guangzhou Chem Ind,2015,(15):148-149.
[12]关于发布化妆品安全技术规范(2015年版)的公告[EB/OL].[2018-7-18].http://scjg.fuzhou.gov.cn/zz/xxgk/fgwj/bljl/201807/t20180724_2535575.htm Notice on the issuance of technical specifications for safety of cosmetics(2015 edition)[EB/OL].[2018-7-18].http://scjg.fuzhou.gov.cn/zz/xxgk/fgwj/bljl/201807/t20180724_2535575.htm
[13]郭好洁,童贵忠,李娜.生物法检测化妆品中防腐剂的防腐效力观察[J].预防医学,2005,17(8):77.Guo HJ,Tong GZ,Li N.Observation on the antiseptic effect of preservatives in cosmetics by biological method[J].Prev Med,2005,17(8):77.
[14]张太军,陈朝茂,刘迪,等.化妆品微生物挑战性实验的优化[J].日用化学品科学,2013,36(5):26-29.Zhang TJ,Chen CM,Liu D,et al.Optimization of cosmetic microbial challenge experiments[J].Deterg Cosmet,2013,36(5):26-29.
[15]林惠芬,李斌,方惠英.用微生物挑战性试验评价化妆品防腐剂效果[J].日用化学工业,1999,(4):43-45.Lin HF,Li B,Fang HY.Evaluation of cosmetic preservative effect by microbiological challenge[J].China Surfact Deterg Cosmet,1999,(4):43-45.
[16]施昌松,蔡晓真,张洪广.化妆品中微生物与防腐体系的构建[J].日用化学品科学,2006,29(12):14-15.Shi CS,Cai XZ,Zhang HG.The construction of microorganism and anti-corrosion system in cosmetics[J].Deterg Cosmet,2006,29(12):14-15.
[17]庄孟芙,向立群,江俊华.山梨坦辛酸酯在个人护理产品中的防腐协同增效作用研究[J].中国洗涤用品工业,2017,(6):39-43.Zhuang MF,Xiang LQ,Jiang JH.Study on the antiseptic synergistic effect of sorbitan octanate in personal care products[J].China Clean Ind Assoc,2017,(6):39-43.
[18]张蓥.食品防腐中生物防腐剂的应用探究[J].食品安全导刊,2018,(6):112-113.Zhang Y.Research on the application of biological preservatives in food preservatives[J].China Food Saf Mag,2018,(6):112-113.