离子色谱法测定合肥市PM2.5微粒中的水溶性阴离子

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英文篇名：Determination of the Water-soluble Anion in PM2.5 by Ion Chromatography in Hefei 作者：付珍 ; 张良璞 ; 吴缨 英文作者：Fu Zhen ; Department of Biological and Environmental Engineering ; Hefei University 关键词：离子色谱法 ; PM2.5 ; 阴离子 ; 合肥市 英文关键词：Ion chromatography ; PM2.5 ; Anion ; Hefei 刊名：安徽农学通报 英文刊名：Anhui Agricultural Science Bulletin 出版日期：2013-10-25 出版单位：安徽农学通报 机构：合肥学院生物与环境工程系;合肥市环境监测中心站;合肥学院化学与材料工程系; 年：2013 期：20 CN：34-1148/S ISSN：1007-7731 页：82-83+129 页数：3 分类号：O657.75;X831 语种：中文; 文件大小：375K

摘要

对合肥市PM2.5膜样品经过剪碎、超纯水浸泡、超声提取后,用离子色谱法对滤液中的阴离子进行测定,加标回收率和相对标准偏差均符合质量控制的要求。该方法检测到合肥市PM2.5中的主要阴离子为F-、Cl-、NO3-、SO42-,检出限分别为0.009 167、0.012 62、0.030 78、0.038 47mg/L,且相关系数都在0.999以上。该测定方法具有高效、高速、高灵敏度和选择性好等优点。
        PM2.5 samples membranes were cut up,immersed in ultrapure water and extracted by ultrasonic in Hefei. Anions in filtrate were detected by ion chromatography. Standard addition recoveries and relative standard deviation were satisfied with the requirement of quality control. The results showed that the main anions in PM2.5were F-、Cl-、NO3-、SO42-in Hefei. Their detection limit were 0.009 167,0.012 62,0.030 78,0.038 47mg/L,respectively. The correlation coefficient of these anion were greater than 0.999. This method had high efficiency,high speed,high sensitivity and good selectivity,etc.

引文

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    [3]钱飞中,李应群.离子色谱法测定TSP中水溶性离子[J].化学分析计量,2002,11(2):18-19.

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